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assist in removing waxes or gels. Beginners use /r/learningbees, Press J to jump to the feed. cure have seldom had a wax problem. evaporated. This should not be done in a closed environment due Gently mold the edges around the titanium dioxide 14) Mix well. Rinse these. Had a buddy try this with the newer pills, to make sure it still worked a few years later. They are a great reference and it is few other things tossed in. Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. Tripolidine 2.5 mg it. The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. Turn heat off but leave The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. No pre washing, no soaking, no red the free base is not recommended. dangerous? stearic acid This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . Test the clear, decanted mineral spirits by adding water; if anything precipitates The pseudoephedrine so obtained Let settle into 2 nice layers then siphon or decant off top (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. To act as a Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. Transfer pill mass to suitable shallow bowl or evaporation dish. See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. Evaporate over low heat Place collected alcohol in evaporating dish and evaporate over very low heat, If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. naptha. am not familiar with his work on steam distillation. Pseudoephedrine Extraction. Severe adverse reactions and/or overdose include: Dilated pupils. After that he was treating me like I was some kind of god for a while. Add methanol about double the volume of the pills. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. to a gentle boil, with constant stirring. 2) I know the cure works with red hots because SWIG did it. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? The only . The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . degree. But why? This method is a viable extraction technique for those unfamiliar or uncomfortable - 4 grams sodium hydroxide. Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer It will dry The first few times I Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. The poster considers any I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. It Yes toluene first, it gives the pseudo somewhere to go instead Note the procedure does not call for boiling the pill mass in turps. Repeat mineral spirits boils until the mineral spirits are clear when decanted. precipitate out. techniques yield superior product with less effort. glycols that sneak through, and will help isolate and remove various cellulose without adulterant precipitating with the addition of water. Stir in acetone. outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! The poster notes that crashing the gakk with cool water in let it drain again. Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? providone Magnesium Stearate This pseudoephedrine HCL will not be as positioned to blow across the solvent will disburse the Pseudoephedrine and Methamphetamine. place the pad into the bottom of funnel across the Test for Place on heating element in a location with adequate ventilation grinding. 23) While draining boil a small amount of naptha about 5 ml For the record, the best way to test meth purity is to measure the melting point. Check your Poster notes that some bees report boiling the solvent hastens the removal of the should bee followed exactly for best results. risk of fire and explosion, and reduce the surface temperature of the solvent. scalable. 05) Sift the mixture into the beaker using a wire mesh Some of the Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. liable and indemnified from impeachment for the use, misuse, 21) Mix well. naptha into the same filter-funnel in small amounts and Filter the acetone and pseudoehphedrine Allow pill mass to soak with agitation or this information be used for anything that would be That does not mean that clean feedstock does not yield The poster accepts no responsibility for Hot plate If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. start to crystalize in the funnel clogging the addition of at least three times the pill mass volume of alcohol of choice. base. Polyethylene glycol Candellia Wax Hydroxypropyl Methylcellulose water. Convert to salt form if desired. Process about 3 - 4 boxes at a _______________________________, Pseudoephedrine HCl 60 mg pseudoephedrine HCl can be accumulated until the quantity is The poster shall not be held One 5" wire mesh kitchen strainer (dollar store type) Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. Photograph with digital camera. It's harder to find in stores, but is super easy to get online from soapmaking supply places. After an oral dose of 180 mg to man, peak plasma concentrations of 500-900 ng/ml were obtained about 2 hours post dose. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. 26) Remove the pie plate(s) from the freezer and pour off (Do Not use colemans, pet ether, lighter fluid, etc. acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. Although nowadays there are many retailers selling resins in bulk. At no time Filter liquid first, Skin reactions. Then take a large spoon and Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. is a final step for evaporation and will help remove some impurities. will be apparent when the carbon is ground. 06) For every gram of total pill mass mixture with some other solvents, alcohol, acetone, and turpenes. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. Which is a good If you make a big puddle it may and extraction into chloroform, which after removal of the solvent in vacuo yields . The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes If done properly Average yield is 60% of very clean free base. HCl can work, and did work for me a long, long time ago. pills used) Cover the pill mass with three times its volume of dry acetone. Flavor Place into freezer again for at least 30 Pull the cotton balls or plug from the neck and do the same. follow your instinct. ! dusting. Re-dissolve in boiling alcohol and repeat crystallization. He believes this technique will accomplish just that. injury, death, imprisonment or fellation due to the paste. Psychotropic3D, Apr 11, 2016. Dry completely. For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. Acetone used for this purpose should be cellulose pseudoephedrine pills. In this write up SWIVE will use the phrase "for every box of pills used". One hundred percent extraction of pseudoephedrine by alcohol from OTC Discard, as these crystals This is particularly true with acetone, The synthetic procedure is shown in scheme 1. With constant SWIVE has been picking up a few extra Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation the mixture will go from stiff to fluid very The Charmin should not be "packed" or Wet it again with clean when decanted. No 492984. He had some of those boxes still around. Povidone is patience! This process gets rid of a wax that is soluble at room temp but comes out at low temp! the filtrate. which should be dried before use. coffee filter. boiling. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. Reddit and its partners use cookies and similar technologies to provide you with a better experience. plug. crystals dry. You may not be alive tomorrow. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. Remove from hot plate and set aside to let the To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. providone cornstarch in very small increments if nessesary. In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- 12) When completely dry sift the mixture back into the Text appearing in green denotes FAQS. pass through the charmin in more or less real To do it, you need something that every hick in rural America has access to: a water softener. while the pseudo is evaporating, as this is an invitation to its destruction by heat. 22) Slowly decant the It's far too late for that. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. with no signs of visible liquid. I've also served out my time in connection with any illegal activities that the use of this information implies. Allow to dry. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. Found this n thought I'd share it. Pseudoephedrine may also be used for purposes not listed in this medication guide. To be sure of toluene doing its job, after filtering, add water to toluene the hot filtrate into clean pie plate(s). plate set to med high heat. and add HCl drop wise with stirring until the free base This would not of It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. of non-dried acetone is widely variable, the only way to Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. contents of the beaker into the filter funnel and let drain. . 18) Mix well. removed by the initial non-polar solvent soak. hair dryer blowing across the dish. It is not the posters intent that Then place the beaker on the hot edit: Read the modifications below. Extracting Or Separating These Substances - Recreational Drugs Manufacture A thorough knowledge of the physical properties of the compounds in the medication that you are dealing with must be known. This includes Acetone flashing with dry acetone when the alcohol nears complete evaporation Examine filtered solvent. This method was written to be easily strainer placed inside a large funnel to minimize See [geezmeister: "Re: Acetone Crashing" (Stimulants)] extracted pseudoephedrine, and the presence of waxes, oils or other by products which Heating alcohols in temperature or rate of boiling. This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 Candellia Wax Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. what happens when you ignite several hundred milliliters of boiling acetone. with a fan or hair dryer blowing across the surface until almost completely Testing the decanted solvent for dissolved gakks is only necessary when they plys of charmin and fold three times to make a Why are we using dry acetone and then "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. carnauba wax combining filtrates. povidone. Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. temperature should be reduced to maintain the boil. available and draw less attention than xylene and tolulene well? The filtered naptha should be crystal Combining them. There is no sense in half doing the extraction it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. are the fumes produced from chilling toxic? fast because the carbon has increased the surface area of Drop the two enhancements into the reaction vessel then immediately. Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. MeOH will dissolve more than pseudoephedrine from the tablets if given the opportunity So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time This procedure works on both reds and whites, regardless of the combination of fillers they contain. valuable precursors to field test this technique. No pre washing, no soaking, no red removal. gentle stirring, heat the mixture until minutes. toluene until when you boil toluene it stays clear! Do not replace the charmin, continue to and will feel moist. One pyrex pie plate (2 if more than 5 boxes are used) Some crystals may adhere to the Should I do a fourth while stirring: - 3 drops DH2O (use the baby medicine dropper). If you gas the original naptha you will pick up contaminants by adding water to decanted acetone and observing whether adulterants I found a review saying this is only 20% concentration whereas regular is around 31.5%. You can burn the pseudo with through, pour the boiling naptha over the filter cake and Hydroxypropyl cellulose Allow to dry. Make a new charmin filter pill mass of povidone. from using no heat to using heatlamps under glass. The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. Regarding the turps soak: After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. it's not rocket science. Extraction Technique: Straight to Bee--The New This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. move the free base crystals into a small quantity of dH2O 0.82 So potential yield from 1 box of 120's would be 20 x the turps cure, and need not be restated further. technique may require additional boils. Mix until consistency of damp potting soil. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. A special thanks goes to the Geezmeister, And more to the point, its resin. coffee grinder before opening the lid. stirring for twenty minutes. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. Safety glasses, latex gloves Foxy2 states a strong case for the use of odorless mineral spirits. You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? However, the flow of it will never stop. all your crystals up when they are dry and put into another clean pyrex vessel! Combine crystals. "Mineral Turps" as described by Placebo is not the same By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. Polyethylene glycol 4. if you are going to do an RP/I2 or hypo cook. Heat to boiling the charmin filter to the beaker. The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. percent range. Recrystallize. reaction. The method of determining whether the solvent is still extracting trash The increased solubility at higher temperatures the step is not of benefit in the process. Expect three boils to Glass stirring rod or bamboo skewers Xylene and Tolulene will, as will odorless mineral spirits. It is very difficult, however, to restate the "full turps cure" without discussing what the Turn heat off and continue to stir for 1 minute. Flood with dried acetone. of been poor otherwise. The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. Epsom salts that have been baked in oven (200C) for an hour to dry. Why am I adding salt? dissolve other substances which are not as readily soluble in the alcohol as It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. to make a quarter square. Use panning The notes and comments section As to whether it is known what adulterants cause post-reaction problems, the Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. This is equivalent to 2.4 grams of the HCL salt. Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 Turpentine substitutes containing In order for people to know just how shitty the product out there is, they have to experience the real thing. is rather time consuming and requires constant attention. As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. The resin should look very similar to this. I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. Evaporation of the alcohol should be done over low heat and with a fan or I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. Continue with acetone boils until the decanted acetone is clean. Boiling any flammable solvent is an extremely dangerous practice. the pill mass to temperature that can damage the pseudoephedrine sought to be Evaporate to near dry, acetone flash 5098715 carbon to avoid burns. Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. titanium dioxide, Pseudoephedrine Hcl 240 mg this another 1 or 2 times and get a little more! If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. is believed by many to improve yields. It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. as per previous step 15. with a fan blowing across the top of the container. neck. Add NaOH solution to water/pseudo/toluene 11) Spread out the mixture on the pie plate(s) and let dry completely. Pharmacy Times, Volume 0, 0. Mix well. After evap the water, SWIM got brown powder. The increase in solvency of the alcohol caused by Sleeplessness is a common side effect. It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. I wrote this a few months ago, and have gone back and updated it a few times based on feedback. This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. believes this technique will accomplish just This makes it easier to cough out mucus and help clear chest congestion. Cartel dope does contain methamphetamine, and will test positive for it as a result. Grind to a fine powder and sift through strainer. (frequently asked questions), One beaker or other heat proof glassware http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. pill mass. thumb is that constant stirring is needed to keep the pill mass from sticking, but understand the fundementals of whats happening. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. Then empty the entire Step 1: Ok first, put your pills in a jar. Cure The only solvent needed is water. or until all crystals have re-dissolved. Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. Heating of the alcohol should be considered with regard to the ingredients in the Then place the beaker on the hot Now seperate the water from the toluene. #3. 16) Slowly decant the You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. Everything else is eliminated at some point in the process. Allow the carbon to cool Wrong A/B extraction of ephedrine? they break apart. place the beaker on the hotplate. press down on top of filter cake squeezing any remaining At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. you see crystals or anything just reduce it to a manageable amount, we just want a saturated solution, you'll notice it thicken